METHOD OF PRODUCING PHENOL
2023-09-28
专利权人AS RUSSIA UFA FEDERAL RES CENT (ASUF-Non-standard)
申请日期2023-09-28
专利号RU2829821-C1
成果简介NOVELTY - Invention relates to synthesis of phenol, which is an important raw material for chemical and pharmaceutical industry. Method of producing phenol is characterized by that phenol is obtained by oxidation of benzene with ammonium persulphate at 45–80 °C in an alkaline medium in the presence of sodium hydroxide and 30 wt.% hydrogen peroxide with molar ratio of benzene:NaOH:PSA:H2O2 equal to 1:3:1.5:1–8, with intensive stirring for 10–15 hours, extraction of intermediate phenyl sulphate by butanol extraction, hydrolysis of the latter with sulfuric acid at 90 °C and extraction of the target compound by extraction with ethanol with output of 31–60%. USE - Organic chemistry. ADVANTAGE - Providing a simple method of producing phenol with increased output of the end product. 1 cl, 1 tbl, 1 ex
IPC 分类号C07C-037/60 ; C07C-039/04
国家俄罗斯
专业领域化学化工
语种英语
成果类型专利
文献类型科技成果
条目标识符http://119.78.100.226:8889/handle/3KE4DYBR/20205
专题中国科学院新疆生态与地理研究所
作者单位
AS RUSSIA UFA FEDERAL RES CENT (ASUF-Non-standard)
推荐引用方式
GB/T 7714
ALPHA B,MUSTAFIN A G,GIMADIEVA A R,et al. METHOD OF PRODUCING PHENOL. RU2829821-C1[P]. 2023.
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