Preparing polyhalocarboxylic acid chloride for applying in preparation of agrochemicals and pharmaceutical intermediates, comprises oxidizing preheated polyhaloalkanes with oxygen and radical initiator to form gaseous mixture, and irradiating in fluorinated ethylene propylene-perfluoralkoxy coil
2023-09-29
专利权人SRF LTD (SRFS-Non-standard)
申请日期2023-09-29
专利号IN202313065415-A
成果简介NOVELTY - Preparing polyhalocarboxylic acid chloride (I), comprises (a) oxidizing preheated polyhaloalkanes (II) with oxygen and a radical initiator to form a gaseous mixture; and (b) irradiating the gaseous mixture in fluorinated ethylene propylene/perfluoralkoxy coil using radiating source to obtain polyhalocarboxylic acid chloride, having more than 99% selectivity. USE - Method for preparing polyhalocarboxylic acid chloride for applying in preparation of agrochemicals and pharmaceutical intermediates. ADVANTAGE - The method prevents the use of highly expensive equipment, and thus reduces overall cost of process, and uses reactor, which helps in improving reaction strength and also helps to avoid the corrosion of reactor, provides efficient recycling and recovery of key reagents, and is efficient and eco-friendly process. DETAILED DESCRIPTION - Preparing polyhalocarboxylic acid chloride of formula (I), comprises (a) oxidizing preheated polyhaloalkanes of formula (II) with oxygen and a radical initiator to form a gaseous mixture; and (b) irradiating the gaseous mixture in fluorinated ethylene propylene/perfluoralkoxy coil using radiating source to obtain polyhalocarboxylic acid chloride, having more than 99% selectivity. R1=fluorinated and/or chlorinated 1-3C alkyl.
IPC 分类号C07C-051/00 ; C07C-051/58 ; C07C-051/60 ; C07C-051/64 ; C07C-053/42 ; C07C-053/50
国家印度
专业领域化学化工
语种英语
成果类型专利
文献类型科技成果
条目标识符http://119.78.100.226:8889/handle/3KE4DYBR/20192
专题中国科学院新疆生态与地理研究所
作者单位
SRF LTD (SRFS-Non-standard)
推荐引用方式
GB/T 7714
ANURAG J,HANUMAN G,PRABHU B,et al. Preparing polyhalocarboxylic acid chloride for applying in preparation of agrochemicals and pharmaceutical intermediates, comprises oxidizing preheated polyhaloalkanes with oxygen and radical initiator to form gaseous mixture, and irradiating in fluorinated ethylene propylene-perfluoralkoxy coil. IN202313065415-A[P]. 2023.
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