Method of producing 6-styryl-4-trifluoromethyl-2-thioxo-1,2-dihydropyridine-3-carbonitriles
2023-11-23
专利权人UNIV CHUVASHIYA (UYCH-Non-standard)
申请日期2023-11-23
专利号RU2827934-C1
成果简介NOVELTY - Invention relates to production of 6-styryl-4-trifluoromethyl-2-thioxo-1,2-dihydropyridine-3-carbonitriles of general formula (1), where R1=H, R2=H, R3=H or R1=H, R2=H, R3=OH, which can be used in photovoltaics, molecular electronics, nonlinear optics, photorefractive devices, laser and sensor equipment, as well as in synthesis of compounds with anticancer, antimicrobial and antiviral properties. Method involves reaction of 6-methyl-2-thioxo-4-trifluoromethyl-1,2-dihydropyridine-3-carbonitrile with benzaldehyde or 4-hydroxybenzaldehyde in 1,4-dioxane medium in the presence of pyrrolidine at temperature of 70–80 °C for 10–12 hours, the reaction mass is diluted with water, acidified with diluted hydrochloric acid and the precipitate is filtered. USE - Organic chemistry. ADVANTAGE - Obtaining target products with output of 69–75%. 1 cl, 2 ex
IPC 分类号C07D-211/90
国家俄罗斯
专业领域材料科学
语种英语
成果类型专利
文献类型科技成果
条目标识符http://119.78.100.226:8889/handle/3KE4DYBR/19197
专题中国科学院新疆生态与地理研究所
作者单位
UNIV CHUVASHIYA (UYCH-Non-standard)
推荐引用方式
GB/T 7714
LIPIN K V,KHAKIMOVA I I,ERSHOVA A I,et al. Method of producing 6-styryl-4-trifluoromethyl-2-thioxo-1,2-dihydropyridine-3-carbonitriles. RU2827934-C1[P]. 2023.
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