METHOD OF PRODUCING TRIS(8-HYDROXYQUINOLINATE)ALUMINIUM
	BELOV D V; BELYAEV S N; PAKHOMOV G L
	2024-04-11
专利权人	SUPERHARD & NEW CARBON MATERIALS INST (SUPE-Non-standard)
申请日期	2024-04-11
专利号	RU2830365-C1
成果简介	NOVELTY - Invention relates to a method of producing tris(8-hydroxyquinolinate)aluminium. Method involves heating aluminium metal powder in an aqueous solution of a base while stirring until intense gas release begins, adding 8-hydroxyquinoline (HQ) in the aqueous solution of the same base with molar ratio Al:HQ = 1:3. Obtained solution is heated and the boiling point is maintained for 60 minutes with constant stirring at a rate of not less than 300 rpm. Obtained precipitate of tris(8-hydroxyquinolinate)aluminium is filtered, washed with water and dried at temperature of 120 °C in an argon atmosphere, after which the obtained precipitate is recrystallised from chloroform. USE - Chemistry. ADVANTAGE - Development of technologically simple and cheap method of obtaining high-purity tris(8-hydroxyquinolinate)aluminium in considerable volumes. 4 cl, 4 dwg
IPC 分类号	C07D-215/30 ; C07F-005/06 ; C09K-011/06
国家	俄罗斯
专业领域	化学化工
语种	英语
成果类型	专利
文献类型	科技成果
条目标识符	http://119.78.100.226:8889/handle/3KE4DYBR/17246
专题	中国科学院新疆生态与地理研究所
作者单位	SUPERHARD & NEW CARBON MATERIALS INST (SUPE-Non-standard)
推荐引用方式 GB/T 7714	BELOV D V,BELYAEV S N,PAKHOMOV G L. METHOD OF PRODUCING TRIS(8-HYDROXYQUINOLINATE)ALUMINIUM. RU2830365-C1[P]. 2024.

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