Method of producing zirconates of rare-earth elements with pyrochlore structure
2024-05-08
专利权人UNIV RUSSIAN TECHNOLOGICAL MIREA (UYRU-Non-standard)
申请日期2024-05-08
专利号RU2830763-C1
成果简介NOVELTY - Invention relates to chemical industry and can be used in production of the main working layer of thermal barrier coatings and technical ceramics when making solid electrolytes, solid oxide fuel cells, gas-analytical sensors. Reaction mixture is prepared which contains, taken in a stoichiometric ratio corresponding to the composition Ln2Zr2O7, the starting compounds: zirconium, which is represented by amorphous hydrated zirconium oxide, and a rare-earth element, which is represented by europium or gadolinium acetate. Obtained reaction mixture is first subjected to microwave treatment with power of 600 W for 15 minutes to obtain europium zirconate Eu2Zr2O7 with a pyrochlore structure or 9 minutes to obtain gadolinium zirconate Gd2Zr2O7 with a pyrochlore structure. Further, thermal treatment of the obtained powder is carried out at temperature of 1,200 °C for 5 hours. USE - Chemistry. ADVANTAGE - Invention provides reduction of synthesis temperature by 100-200 °C and duration by 1-2 hours when producing zirconates of said rare-earth elements with a pyrochlore structure. 1 cl, 2 dwg, 2 ex
IPC 分类号C01F-017/10 ; C01F-017/30 ; C01G-025/00
国家俄罗斯
专业领域材料科学
语种英语
成果类型专利
文献类型科技成果
条目标识符http://119.78.100.226:8889/handle/3KE4DYBR/16820
专题中国科学院新疆生态与地理研究所
作者单位
UNIV RUSSIAN TECHNOLOGICAL MIREA (UYRU-Non-standard)
推荐引用方式
GB/T 7714
NIKISHINA E E,GRECHISHNIKOV N V,VOLCHKOVA E V,et al. Method of producing zirconates of rare-earth elements with pyrochlore structure. RU2830763-C1[P]. 2024.
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